{"id":5451,"date":"2022-08-12T12:25:35","date_gmt":"2022-08-12T12:25:35","guid":{"rendered":"https:\/\/longchangchemical.com\/?p=5451"},"modified":"2022-08-12T12:25:35","modified_gmt":"2022-08-12T12:25:35","slug":"introduction-and-principles-of-common-laboratory-instrument-analysis","status":"publish","type":"post","link":"https:\/\/longchangchemical.com\/tr\/introduction-and-principles-of-common-laboratory-instrument-analysis\/","title":{"rendered":"Genel laboratuvar cihaz analizlerinin tan\u0131t\u0131m\u0131 ve prensipleri"},"content":{"rendered":"

Genel laboratuvar cihaz analizlerinin tan\u0131t\u0131m\u0131 ve prensipleri<\/strong><\/h1>\n

1. K\u0131z\u0131l\u00f6tesi so\u011furma spektrometresi, IR<\/p>\n

Analitik prensip: K\u0131z\u0131l\u00f6tesi \u0131\u015f\u0131k enerjisinin emilmesi, de\u011fi\u015fen dipol momentleri ile molek\u00fcllerin titre\u015fimsel, rotasyonel enerji seviyesi s\u0131\u00e7ramalar\u0131na neden olur.<\/p>\n

Spektrumun g\u00f6sterimi: iletilen \u0131\u015f\u0131k enerjisinin iletilen \u0131\u015f\u0131\u011f\u0131n frekans\u0131 ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: fonksiyonel gruplar\u0131n veya kimyasal ba\u011flar\u0131n karakteristik titre\u015fim frekanslar\u0131n\u0131 sa\u011flayan piklerin konumu, yo\u011funlu\u011fu ve \u015fekli.<\/p>\n

2. Ultraviyole absorpsiyon spektrometresi, UV<\/p>\n

Analiz prensibi: UV enerjisinin emilmesi, molek\u00fcldeki elektron enerji seviyesinde bir s\u0131\u00e7ramaya neden olur.<\/p>\n

Spektrumun g\u00f6sterimi: absorbe edilen \u0131\u015f\u0131\u011f\u0131n dalga boyu ile g\u00f6receli absorbe edilen \u0131\u015f\u0131k enerjisinin de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: molek\u00fcldeki farkl\u0131 elektronik yap\u0131lar hakk\u0131nda bilgi sa\u011flayan absorpsiyon piklerinin yeri, yo\u011funlu\u011fu ve \u015fekli.<\/p>\n

3. N\u00fckleer manyetik rezonans spektrometresi, NMR<\/p>\n

Analiz prensibi: Harici bir manyetik alanda n\u00fckleer manyetik momentlere sahip \u00e7ekirdekler, radyo frekans\u0131 enerjisini emer ve n\u00fckleer spin enerji seviyelerinde s\u0131\u00e7ramalar \u00fcretir.<\/p>\n

Spektrumun g\u00f6sterimi: absorbe edilen \u0131\u015f\u0131k enerjisinin kimyasal kayma ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: kimyasal kaymalar, yo\u011funluklar, b\u00f6l\u00fcnme fraksiyonlar\u0131 ve piklerin ba\u011flant\u0131 sabitleri, \u00e7ekirdek say\u0131s\u0131, bulunduklar\u0131 kimyasal ortam ve geometrik konfig\u00fcrasyonlar\u0131 hakk\u0131nda bilgi sa\u011flar.<\/p>\n

4. Floresan spektrometresi, FS.<\/p>\n

Analiz prensibi: Elektromanyetik radyasyonla uyar\u0131ld\u0131ktan sonra, *d\u00fc\u015f\u00fck tek hatl\u0131 uyar\u0131lm\u0131\u015f durumdan tek hatl\u0131 temel duruma geri d\u00f6nen floresan emisyonu.<\/p>\n

Spektrumun g\u00f6sterimi: yay\u0131lan floresan enerjisinin \u0131\u015f\u0131\u011f\u0131n dalga boyu ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: floresan verimlili\u011fi ve \u00f6mr\u00fc, molek\u00fcldeki farkl\u0131 elektronik yap\u0131lar hakk\u0131nda bilgi sa\u011flar.<\/p>\n

5. Raman spektrometresi, Ram.<\/p>\n

Analiz prensibi: I\u015f\u0131k enerjisinin emilmesi, polarizasyon oran\u0131nda bir de\u011fi\u015fiklikle molek\u00fcllerin titre\u015fimlerine neden olur ve Raman sa\u00e7\u0131lmas\u0131 \u00fcretir.<\/p>\n

Spektrumun g\u00f6sterimi: sa\u00e7\u0131lan \u0131\u015f\u0131k enerjisinin Raman kaymas\u0131 ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: fonksiyonel gruplar\u0131n veya kimyasal ba\u011flar\u0131n karakteristik titre\u015fim frekanslar\u0131n\u0131 sa\u011flayan piklerin konumu, yo\u011funlu\u011fu ve \u015fekli.<\/p>\n

6. K\u00fctle spektrometresi analiz\u00f6r\u00fc, MS.<\/p>\n

Analitik prensip: molek\u00fcller vakumda elektronlarla bombard\u0131mana tutulur ve farkl\u0131 m\/e'lerde elektromanyetik alanlar taraf\u0131ndan ayr\u0131lan iyonlar olu\u015fturur.<\/p>\n

Spektrumun g\u00f6sterimi: m\/e ile bir \u00e7ubuk grafik olarak iyonlar\u0131n g\u00f6receli bas\u0131kl\u0131\u011f\u0131.<\/p>\n

Sa\u011flanan bilgiler: molek\u00fcler iyonlar\u0131n ve fragman iyonlar\u0131n\u0131n k\u00fctle say\u0131s\u0131 ve bunlar\u0131n g\u00f6receli bas\u0131kl\u0131\u011f\u0131, molek\u00fcler a\u011f\u0131rl\u0131k, elemental bile\u015fim ve yap\u0131 hakk\u0131nda bilgi sa\u011flar.<\/p>\n

7. Gaz kromatografisi, GC.<\/p>\n

Analiz prensibi: farkl\u0131 b\u00f6lme katsay\u0131lar\u0131 nedeniyle numunenin bile\u015fenlerinin hareketli ve sabit fazlar aras\u0131nda ayr\u0131lmas\u0131.<\/p>\n

Spektrumun g\u00f6sterimi: kolon sonras\u0131 at\u0131k konsantrasyonunun al\u0131konma de\u011feri ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: pikin al\u0131konma de\u011feri bile\u015fenlerin termodinamik parametreleri ile ilgilidir ve nitel temeldir; pik alan\u0131 bile\u015fen i\u00e7eri\u011fi ile ilgilidir.<\/p>\n

8. elektron paramanyetik rezonans spektrometresi, ESR.<\/p>\n

Analitik prensip: RF enerjisinin harici bir manyetik alanda molek\u00fcllerdeki e\u015fle\u015fmemi\u015f elektronlar taraf\u0131ndan emilmesi, elektron spin enerji seviyesi s\u0131\u00e7ramalar\u0131na neden olur.<\/p>\n

Spektrumun g\u00f6sterimi: absorbe edilen \u0131\u015f\u0131k enerjisinin veya diferansiyel enerjinin manyetik alan g\u00fcc\u00fc ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: spektral \u00e7izgi konumlar\u0131, yo\u011funluklar, b\u00f6l\u00fcnme say\u0131s\u0131 ve hiperfine b\u00f6l\u00fcnme sabitleri, e\u015fle\u015fmemi\u015f elektron yo\u011funluklar\u0131, molek\u00fcler ba\u011flanma \u00f6zellikleri ve geometrik konfig\u00fcrasyonlar hakk\u0131nda bilgi sa\u011flar.<\/p>\n

9. B\u00f6l\u00fcnme gaz kromatograf\u0131, PGC.<\/p>\n

Analitik prensip: belirli \u00f6zelliklere sahip par\u00e7alar elde etmek i\u00e7in polimerik malzemelerin belirli ko\u015fullar alt\u0131nda anl\u0131k olarak b\u00f6l\u00fcnmesi.<\/p>\n

Spektrumun g\u00f6sterimi: kolon sonras\u0131 at\u0131k konsantrasyonunun al\u0131konma de\u011feri ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: spektrumun parmak izi veya karakteristik par\u00e7alanma pikleri, polimerin kimyasal yap\u0131s\u0131n\u0131 ve geometrik konfig\u00fcrasyonunu karakterize eder.<\/p>\n

10 . Jel kromatografisi, GPC.<\/p>\n

Analiz prensibi: numunenin jel kolon boyunca molek\u00fcllerin hidrodinamik hacmine g\u00f6re ayr\u0131lmas\u0131, daha b\u00fcy\u00fck molek\u00fcllerin \u00f6nce d\u0131\u015far\u0131 akmas\u0131.<\/p>\n

Spektrumun g\u00f6sterimi: kolon sonras\u0131 at\u0131k konsantrasyonunun al\u0131konma de\u011feri ile de\u011fi\u015fimi.<\/p>\n

Sa\u011flanan bilgiler: polimerlerin ortalama molek\u00fcler a\u011f\u0131rl\u0131\u011f\u0131 ve da\u011f\u0131l\u0131m\u0131.<\/p>\n

11. Ters gaz kromatografisi, IGC.<\/p>\n

Analitik prensip: Prob molek\u00fcl\u00fcn\u00fcn al\u0131konma de\u011ferinin, molek\u00fcl ile sabit faz olarak polimer numune aras\u0131ndaki etkile\u015fim kuvvetlerine ba\u011fl\u0131 olarak de\u011fi\u015fmesi.<\/p>\n

Spektrumun g\u00f6sterimi: Prob molek\u00fcl\u00fcn\u00fcn spesifik al\u0131konma hacminin logaritmas\u0131n\u0131n kolon s\u0131cakl\u0131\u011f\u0131n\u0131n tersi ile de\u011fi\u015fim e\u011frisi.<\/p>\n

Sa\u011flanan bilgiler: Prob molek\u00fcl\u00fcn\u00fcn s\u0131cakl\u0131\u011fa kar\u015f\u0131 tutma de\u011feri, polimerin termodinamik parametrelerini sa\u011flar.<\/p>\n

12. Termogravimetri, TG.<\/p>\n

Analiz prensibi: S\u0131cakl\u0131k kontroll\u00fc bir ortamda numune a\u011f\u0131rl\u0131\u011f\u0131n\u0131n s\u0131cakl\u0131k veya zamanla de\u011fi\u015fimi.<\/p>\n

Spektrumun g\u00f6sterimi: numunenin a\u011f\u0131rl\u0131k fraksiyonunun s\u0131cakl\u0131k veya zamanla e\u011frisi.<\/p>\n

Sa\u011flanan bilgiler: e\u011frinin dik d\u00fc\u015f\u00fc\u015f\u00fc numunenin a\u011f\u0131rl\u0131k kayb\u0131 b\u00f6lgesidir ve plato b\u00f6lgesi numunenin termal stabilite b\u00f6lgesidir.<\/p>\n

13. statik termal kuvvet analiz\u00f6r\u00fc, TMA.<\/p>\n

Analiz prensibi: s\u0131cakl\u0131k veya zaman\u0131n bir fonksiyonu olarak sabit bir kuvvetin etkisi alt\u0131nda numunenin deformasyonu.<\/p>\n

Spektrumun g\u00f6sterimi: numunenin deformasyon de\u011ferlerinin s\u0131cakl\u0131k veya zamanla e\u011frisi.<\/p>\n

Sa\u011flanan bilgiler: termal ge\u00e7i\u015f s\u0131cakl\u0131\u011f\u0131 ve mekanik durum.<\/p>\n

14. Diferansiyel Termal Analiz\u00f6r, DTA.<\/p>\n

Analitik prensip: numune ve referans ayn\u0131 s\u0131cakl\u0131k kontroll\u00fc ortamdad\u0131r ve ikisinin farkl\u0131 termal iletkenli\u011fi nedeniyle s\u0131cakl\u0131k fark\u0131 olu\u015fur ve ortam s\u0131cakl\u0131\u011f\u0131 veya zamanla s\u0131cakl\u0131ktaki de\u011fi\u015fim kaydedilir.<\/p>\n

Spektrumun g\u00f6sterimi: ortam s\u0131cakl\u0131\u011f\u0131 veya zaman ile s\u0131cakl\u0131k fark\u0131 e\u011frisi.<\/p>\n

Sa\u011flanan bilgiler: polimerin termal ge\u00e7i\u015f s\u0131cakl\u0131\u011f\u0131 ve \u00e7e\u015fitli termal etkiler hakk\u0131nda bilgi sa\u011flar.<\/p>\n

15. Diferansiyel taramal\u0131 kalorimetri analiz\u00f6r\u00fc, DSC.<\/p>\n

Analitik prensip: numune ve referans ayn\u0131 s\u0131cakl\u0131k kontroll\u00fc ortamdad\u0131r ve s\u0131cakl\u0131k fark\u0131n\u0131 s\u0131f\u0131rda tutmak i\u00e7in gereken enerji de\u011fi\u015fimi ortam s\u0131cakl\u0131\u011f\u0131 veya zaman ile kaydedilir.<\/p>\n

Spektrumun g\u00f6sterimi: \u0131s\u0131n\u0131n e\u011frisi veya ortam s\u0131cakl\u0131\u011f\u0131 veya zaman ile de\u011fi\u015fim oran\u0131.<\/p>\n

Sa\u011flanan bilgiler: polimerin termal ge\u00e7i\u015f s\u0131cakl\u0131\u011f\u0131 ve \u00e7e\u015fitli termal etkiler hakk\u0131nda bilgi sa\u011flar<\/p>\n

16. dinamik termal kuvvet analiz\u00f6r\u00fc, DMA.<\/p>\n

Analiz prensibi: periyodik olarak de\u011fi\u015fen bir d\u0131\u015f kuvvetin etkisi alt\u0131nda numunenin deformasyonunun s\u0131cakl\u0131kla de\u011fi\u015fimi.<\/p>\n

Spektrumun g\u00f6sterimi: s\u0131cakl\u0131k ile mod\u00fcl veya tan\u03b4 e\u011frisi.<\/p>\n

Sa\u011flanan bilgiler: termal ge\u00e7i\u015f s\u0131cakl\u0131\u011f\u0131 mod\u00fcl\u00fc ve tan\u03b4.<\/p>","protected":false},"excerpt":{"rendered":"

Yayg\u0131n laboratuvar cihaz analizinin tan\u0131t\u0131m\u0131 ve ilkeleri 1.K\u0131z\u0131l\u00f6tesi absorpsiyon spektrometresi, IR Analitik prensip: de\u011fi\u015fen dipol momentleri ile molek\u00fcllerin titre\u015fimsel, rotasyonel enerji seviyesi s\u0131\u00e7ramalar\u0131na neden olan k\u0131z\u0131l\u00f6tesi \u0131\u015f\u0131k enerjisinin emilmesi. Spektrumun g\u00f6sterimi: iletilen \u0131\u015f\u0131\u011f\u0131n frekans\u0131 ile ba\u011f\u0131l iletilen \u0131\u015f\u0131k enerjisinin de\u011fi\u015fimi. Sa\u011flanan bilgiler: tepe noktalar\u0131n\u0131n yeri, yo\u011funlu\u011fu ve \u015fekli, [...]<\/p>","protected":false},"author":1,"featured_media":5452,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[106],"tags":[],"class_list":["post-5451","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-laboratory-news"],"yoast_head":"\nIntroduction and principles of common laboratory instrument analysis - Longchang Chemical<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangchemical.com\/tr\/introduction-and-principles-of-common-laboratory-instrument-analysis\/\" \/>\n<meta property=\"og:locale\" content=\"tr_TR\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Introduction and principles of common laboratory instrument analysis - Longchang Chemical\" \/>\n<meta property=\"og:description\" content=\"Introduction and principles of common laboratory instrument analysis 1.Infrared absorption spectrometer, IR Analytical principle: absorption of infrared light energy, causing vibrational, rotational energy level jumps of molecules with changing dipole moments. 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Representation of the spectrum: variation of relative transmitted light energy with frequency of transmitted light. 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