{"id":4885,"date":"2021-12-08T12:34:41","date_gmt":"2021-12-08T12:34:41","guid":{"rendered":"https:\/\/longchangchemical.com\/?p=4885"},"modified":"2026-04-28T10:41:52","modified_gmt":"2026-04-28T10:41:52","slug":"cpba-and-dmf-no-together","status":"publish","type":"post","link":"https:\/\/longchangchemical.com\/tr\/cpba-and-dmf-no-together\/","title":{"rendered":"m-CPBA ve DMF birlikte reaksiyona girdi\u011finde patlama riski vard\u0131r"},"content":{"rendered":"<!-- lc-qa-start -->\n<p><strong>H\u0131zl\u0131 cevap:<\/strong> Surface-control additives are usually selected by defect type, compatibility, and dosage window. The strongest commercial choice is the one that fixes the real problem without creating a new one.<\/p>\n<!-- lc-qa-end -->\n\n\n<p>DMF, organik sentezlerde en yayg\u0131n kullan\u0131lan \u00e7\u00f6z\u00fcc\u00fclerden biridir ve evrensel bir \u00e7\u00f6z\u00fcc\u00fc olarak da bilinir. Bug\u00fcn sizlerle bir reaksiyon vakas\u0131n\u0131 payla\u015faca\u011f\u0131m. m-CPBA ve DMF'nin birlikte kullan\u0131m\u0131 da potansiyel olarak tehlikelidir. m-CPBA, m-kloroperoksibenzoik asit olarak da bilinir ve organik kimyada \u00e7ok yayg\u0131n olarak kullan\u0131lan bir organik oksidan t\u00fcr\u00fcd\u00fcr. Nispeten g\u00fcvenli oldu\u011fu s\u00f6ylenebilir. Ancak kimya alan\u0131 bilinmeyenlerle doludur. Bug\u00fcn payla\u015f\u0131lan literat\u00fcrde bildirilen bir kaza, m-CPBA ve DMF'nin kar\u0131\u015f\u0131k kullan\u0131m\u0131yla ilgilidir ve a\u015fa\u011f\u0131daki kimyasal d\u00f6n\u00fc\u015f\u00fcmlerle do\u011frudan ili\u015fkilidir.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"387\" height=\"92\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/1.jpg\" alt=\"\" class=\"wp-image-4886\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/1.jpg 387w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/1-300x71.jpg 300w\" sizes=\"(max-width: 387px) 100vw, 387px\" \/><\/figure>\n\n\n\n<p>Japonya'daki Fujisawa \u0130la\u00e7 \u015eirketi sentezcileri, pilot \u00f6l\u00e7ekte \u00e7\u00f6z\u00fcc\u00fc olarak DMF kullanarak s\u00fclf\u00fcr\u00fc s\u00fclfokside oksitlemek i\u00e7in m-CPBA kulland\u0131. Sentezleyiciler \u00f6nce 6,3 litre DMF ve 11,0 kg m-CPBA'y\u0131 kar\u0131\u015ft\u0131rd\u0131 ve ikisini 2 saat boyunca kar\u0131\u015ft\u0131rd\u0131. Sistemde \u00e7\u00f6z\u00fcnmeyen madde olu\u015fur ve ard\u0131ndan berrak bir \u00e7\u00f6zelti elde etmek i\u00e7in s\u00fcz\u00fcl\u00fcr ve berrak \u00e7\u00f6zelti organik reaksiyon \u00e7\u00f6zeltisine eklenir. Damlatma i\u015flemi 1 saat boyunca ger\u00e7ekle\u015ftirildi\u011finde, m-CPBA'n\u0131n DMF \u00e7\u00f6zeltisi aniden y\u00fckselir ve gaz a\u00e7\u0131\u011fa \u00e7\u0131kar. Ve sonra aniden patlad\u0131. Bu makalenin yazar\u0131 (Org. Proc. Res. Dev.) reaksiyon s\u00fcrecini a\u015fa\u011f\u0131daki \u015fekilde k\u0131saca anlatmaktad\u0131r.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"392\" height=\"119\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/2.jpg\" alt=\"\" class=\"wp-image-4887\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/2.jpg 392w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/2-300x91.jpg 300w\" sizes=\"(max-width: 392px) 100vw, 392px\" \/><\/figure>\n\n\n\n<p>Sentetik personel derhal kazan\u0131n ve patlaman\u0131n nedenini ara\u015ft\u0131rd\u0131. Bunun muhtemelen \u00e7\u00f6z\u00fcnmeyen maddeden kaynakland\u0131\u011f\u0131n\u0131 ve \u00e7\u00f6z\u00fcnmeyen maddenin tam olarak m-CBPO oldu\u011funu tahmin ettiler. Bu \u00e7\u00f6z\u00fcnmeyen madde, hammadde m-CPBA'n\u0131n kendisinden kaynaklanan bir safs\u0131zl\u0131k olabilir veya reaksiyon sisteminde kademeli olarak \u00fcretilebilir. Bu makalenin yazar\u0131 bir dizi do\u011frulama deneyi yapmaya devam etmi\u015ftir. Yazar, m-CPBA hammaddesindeki m-CBPO i\u00e7eri\u011finin sadece 0,2% oldu\u011funu bulmu\u015ftur. Ayr\u0131ca, DTA ve IST deneyleri m-CPBA'n\u0131n 89 derecede eridi\u011fini ve 97 derecenin alt\u0131nda kararl\u0131 oldu\u011funu do\u011frulam\u0131\u015ft\u0131r. Yazar daha sonra m-CPBA'n\u0131n DMF \u00e7\u00f6zeltisi \u00fczerinde bir DTA \u00e7al\u0131\u015fmas\u0131 y\u00fcr\u00fctm\u00fc\u015f ve sonu\u00e7lar m-CPBA'n\u0131n ayr\u0131\u015fma s\u0131cakl\u0131\u011f\u0131n\u0131n 83 derece oldu\u011funu g\u00f6stermi\u015ftir. Yukar\u0131daki deneyler, DMF'nin m-CPBA'n\u0131n kritik ayr\u0131\u015fma s\u0131cakl\u0131\u011f\u0131 noktas\u0131n\u0131 b\u00fcy\u00fck \u00f6l\u00e7\u00fcde etkileyebilece\u011fini g\u00f6stermektedir. Bu nedenle yazar, DMF \u00e7\u00f6z\u00fcc\u00fcs\u00fcn\u00fcn bu kazada \u00f6nemli bir rol oynad\u0131\u011f\u0131na inanmaktad\u0131r.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/3-1.jpg\" alt=\"\" class=\"wp-image-4889\"\/><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"472\" height=\"422\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/4.jpg\" alt=\"\" class=\"wp-image-4890\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/4.jpg 472w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/4-300x268.jpg 300w\" sizes=\"(max-width: 472px) 100vw, 472px\" \/><\/figure>\n\n\n\n<p>Yazar daha sonra, s\u0131cakl\u0131k artt\u0131k\u00e7a m-CBPO i\u00e7eri\u011finin \u00f6nemli \u00f6l\u00e7\u00fcde artt\u0131\u011f\u0131n\u0131 ve DTA ara\u015ft\u0131rmas\u0131n\u0131n, s\u0131cakl\u0131k 125 dereceden fazla oldu\u011funda \u00e7ok ciddi bir patlaman\u0131n \u00f6ng\u00f6r\u00fclebilece\u011fini g\u00f6sterdi\u011fini tespit etti.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"452\" height=\"311\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/5.jpg\" alt=\"\" class=\"wp-image-4891\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/5.jpg 452w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/5-300x206.jpg 300w\" sizes=\"(max-width: 452px) 100vw, 452px\" \/><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"466\" height=\"408\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/6.jpg\" alt=\"\" class=\"wp-image-4893\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/6.jpg 466w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/6-300x263.jpg 300w\" sizes=\"(max-width: 466px) 100vw, 466px\" \/><\/figure>\n\n\n\n<p>Yazar daha sonra m-CPBA DMF \u00e7\u00f6zeltisinin ARC \u00e7al\u0131\u015fmas\u0131n\u0131, konsantrasyon \u00e7al\u0131\u015fmas\u0131n\u0131 ve m-CPBA ve m-CPBO'nun kar\u0131\u015f\u0131k stabilite \u00e7al\u0131\u015fmas\u0131n\u0131 ger\u00e7ekle\u015ftirmi\u015ftir. Nihai sonu\u00e7, m-CPBA DMF \u00e7\u00f6zeltisinin 26 dereceden 70 dereceye yava\u015f\u00e7a y\u00fckselmesinin 185 dakika s\u00fcrd\u00fc\u011f\u00fc ve daha sonra birka\u00e7 dakika veya benzeri bir s\u00fcrede h\u0131zla 200 dereceye y\u00fckselece\u011fidir. Buna ek olarak, daha konsantre m-CPBA DMF \u00e7\u00f6zeltisi daha h\u0131zl\u0131 \u0131s\u0131n\u0131r. m-CPBA ve m-CPBO'nun kar\u0131\u015f\u0131k deneyi, s\u0131cakl\u0131\u011f\u0131n ba\u015flang\u0131\u00e7ta yava\u015f\u00e7a y\u00fckseldi\u011fini, ancak sadece 95 dakika sonra keskin bir s\u0131cakl\u0131k art\u0131\u015f\u0131 olaca\u011f\u0131n\u0131 g\u00f6stermektedir.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"494\" height=\"891\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/7.jpg\" alt=\"\" class=\"wp-image-4895\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/7.jpg 494w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/7-166x300.jpg 166w\" sizes=\"(max-width: 494px) 100vw, 494px\" \/><\/figure>\n\n\n\n<p>\u00d6zet olarak, bu makalenin yazar\u0131 patlaman\u0131n genel s\u00fcrecini vermektedir. \u0130lk olarak, m-CPBO olu\u015fumu s\u0131cakl\u0131kta bir art\u0131\u015fa yol a\u00e7ar ve daha sonra b\u00fcy\u00fck miktarda m-CPBO olu\u015fumu y\u00fcksek s\u0131cakl\u0131klarda bir patlamaya neden olur. Sonunda yazar, bu sorunu ba\u015far\u0131yla \u00e7\u00f6zmek i\u00e7in \u00e7\u00f6z\u00fcc\u00fc olarak diklorometan DCM kullanm\u0131\u015ft\u0131r. DTA deneyleri, \u00e7\u00f6z\u00fcc\u00fc olarak diklorometan kullan\u0131ld\u0131\u011f\u0131nda, zamanla ekzoterm olmad\u0131\u011f\u0131n\u0131 g\u00f6stermektedir.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img decoding=\"async\" width=\"466\" height=\"312\" src=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/10-1.jpg\" alt=\"\" class=\"wp-image-4896\" srcset=\"https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/10-1.jpg 466w, https:\/\/longchangchemical.com\/wp-content\/uploads\/2021\/12\/10-1-300x201.jpg 300w\" sizes=\"(max-width: 466px) 100vw, 466px\" \/><\/figure>\n\n\n\n<p>On binlerle deney yap\u0131n, \u00f6nce g\u00fcvenlik! <strong><a href=\"https:\/\/longchangchemical.com\/tr\/product\/dimethyl-sulfoxide-cas-67-68-5\/\" target=\"_blank\" rel=\"noreferrer noopener\">DMSO<\/a><\/strong> ve DMF g\u00fc\u00e7l\u00fc polar \u00e7\u00f6z\u00fcc\u00fclerdir, organikler i\u00e7in iyi \u00e7\u00f6z\u00fcn\u00fcrl\u00fc\u011fe sahip olmalar\u0131na ra\u011fmen, ayn\u0131 zamanda iki ucu keskin k\u0131l\u0131\u00e7t\u0131rlar!<\/p>\n\n\n<!-- lc-commercial-start -->\n<h2>How buyers usually evaluate coating and ink additives<\/h2>\n<p>Additive selection is usually most effective when the team defines the defect first and then screens compatibility, dosage range, and process stage. That is often much more reliable than choosing only by chemistry family or by a single dramatic lab result.<\/p>\n<ul>\n<li><strong>Start from the defect, not the additive name:<\/strong> wetting loss, crater, microfoam, and instability often need different solutions even inside the same formula.<\/li>\n<li><strong>Check compatibility at the intended dosage:<\/strong> the strongest additive can still be the wrong commercial choice if it narrows the process window too much.<\/li>\n<li><strong>Review the stage of use:<\/strong> some products are most useful during grind, while others matter more during let-down, filling, or final application.<\/li>\n<li><strong>Balance cure or film quality with defect control:<\/strong> the right additive fixes the problem without sacrificing adhesion, gloss, or appearance.<\/li>\n<\/ul>\n<h3>\u00d6nerilen \u00fcr\u00fcn referanslar\u0131<\/h3>\n<ul>\n<li><strong><a href=\"https:\/\/longchangchemical.com\/tr\/product\/chlumiaf-094\/\">CHLUMIAF 094<\/a>:<\/strong> Su bazl\u0131 kaplamalar ve bir\u00e7ok genel k\u00f6p\u00fck kontrol ekran\u0131 i\u00e7in dengeli bir k\u00f6p\u00fck giderici referans\u0131.<\/li>\n<li><strong><a href=\"https:\/\/longchangchemical.com\/tr\/product\/chlumiaf-3062\/\">CHLUMIAF 3062<\/a>:<\/strong> Bask\u0131 m\u00fcrekkebi ve UV m\u00fcrekkebi uyumlulu\u011funun k\u00f6p\u00fck giderici ekranda \u00f6nemli oldu\u011fu durumlarda kullan\u0131\u015fl\u0131d\u0131r.<\/li>\n<li><strong><a href=\"https:\/\/longchangchemical.com\/tr\/product\/chlumiaf-3037\/\">CHLUMIAF 3037<\/a>:<\/strong> Daha sert ko\u015fullarda bile kal\u0131c\u0131 k\u00f6p\u00fc\u011f\u00fcn \u00fcstesinden gelmek i\u00e7in daha g\u00fc\u00e7l\u00fc bir proses-k\u00f6p\u00fck giderme se\u00e7ene\u011fi.<\/li>\n<li><strong><a href=\"https:\/\/longchangchemical.com\/tr\/product\/chlumiwe-3280\/\">CHLUMIWE 3280<\/a>:<\/strong> A strong wetting-agent reference for inks, coatings, and difficult substrate wetting.<\/li>\n<\/ul>\n<h3>Al\u0131c\u0131lar ve form\u00fclat\u00f6rler i\u00e7in SSS<\/h3>\n<p><strong>Why does an additive that looks powerful in a beaker sometimes fail in production?<\/strong><br \/>Because shear, temperature, substrate, and the full formula can all change the way the additive performs under real process conditions.<\/p>\n<p><strong>Should the most aggressive additive always be preferred?<\/strong><br \/>Not usually. The best additive is the one that solves the real defect while preserving the broadest safe operating window.<\/p>\n<!-- lc-commercial-end -->","protected":false},"excerpt":{"rendered":"<p>DMF is one of the most widely used solvents in organic synthesis, and is also known as a universal solvent. Today I will share a reaction case with you. The<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[106],"tags":[],"class_list":["post-4885","post","type-post","status-publish","format-standard","hentry","category-laboratory-news"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.3.1 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>There is a risk of explosion when m-CPBA and DMF react together - Longchang Chemical<\/title>\n<meta name=\"description\" content=\"DMF is one of the most widely used solvents in organic synthesis, and is also known as a universal solvent. 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