{"id":5369,"date":"2022-07-12T13:32:13","date_gmt":"2022-07-12T13:32:13","guid":{"rendered":"https:\/\/longchangchemical.com\/?p=5369"},"modified":"2024-12-11T15:43:47","modified_gmt":"2024-12-11T15:43:47","slug":"brief-description-of-hydrogen-capturing-photoinitiators","status":"publish","type":"post","link":"https:\/\/longchangchemical.com\/nl\/brief-description-of-hydrogen-capturing-photoinitiators\/","title":{"rendered":"Korte beschrijving van waterstofvangende fotoinitiatoren en hun twee hoofdcategorie\u00ebn"},"content":{"rendered":"

Korte beschrijving van waterstofvangende fotoinitiatoren en hun twee hoofdcategorie\u00ebn<\/strong><\/h1>\n

Waterstofvangende fotoinitiatoren, ook bekend als type II fotoinitiatoren, worden over het algemeen gedomineerd door aromatische ketonstructuren en omvatten ook bepaalde aromatische koolwaterstoffen met dikke ringen. Ze hebben bepaalde lichtabsorberende eigenschappen en de bijbehorende co-initiator, d.w.z. waterstofdonor, heeft zelf geen absorptie in het langegolf UV-bereik. Waterstofvangende fotoinitiatoren absorberen UV-energie en bimoleculaire interactie met de co-initiator in de aangeslagen toestand om reactieve radicalen te produceren. Tertiaire aminen worden vaak gebruikt als co-initiatoren voor koppeling met waterstofvangende fotoinitiatoren. Het volgende diagram neemt benzofenon fotoinitiator als voorbeeld om het actieproces te beschrijven.<\/p>\n

 <\/p>\n

Ten eerste, benzofenon + tertiair amine fotoinitiator systeem<\/p>\n

Benzofenon (BP) fotoinitiator is over het algemeen kleurloos of licht gele kristallen, oplosbaarheid in gewone oplosmiddelen is relatief goed, de maximale absorptie golflengte van ongeveer 340nm, en de medium-druk kwiklamp emissie golflengte overeenkomen. Hier moeten we aandacht besteden aan het verschil tussen benzofenon fotoinitiator en benzofenon UV-absorber, hun structuur is relatief vergelijkbaar, de maximale absorptie golflengte van benzofenon UV-absorber is over het algemeen rond de 330 nm. De synthese van BP is eenvoudig, het is een goedkope fotoinitiator, maar de fotoiniti\u00ebrende activiteit is over het algemeen niet zo goed als die van HMPP, HCPK en andere veelgebruikte fotoinitiatoren. De uithardingssnelheid van fotoinitiatoren van het BP-type is relatief traag en het is gemakkelijk om vergeling van de uitgeharde coating te veroorzaken, en de vergeling wordt verergerd door het gebruik van grote hoeveelheden tertiaire amine co-initiatoren.<\/p>\n

 <\/p>\n

Als fotoinitiator voor het vastleggen van waterstof heeft BP ook voordelen. Ten eerste kunnen de lage kosten en de lage prijs worden gebruikt in sommige formuleringen met een lage toegevoegde waarde en lage kwaliteitseisen. Zoals decoratieve snap coatings en gekleurde substraatlakcoatings. Om de kosten, vergeling, uithardingssnelheid en andere factoren in evenwicht te brengen, wordt BP vaak gebruikt in combinatie met andere krakende fotoinitiatoren, BP en actieve amine combinatietoepassing, actieve amine heeft de functie van antioxidant polymerisatie, dus het oppervlak van BP + actieve amine systeem antioxidant polymerisatie effect is beter. Er moet echter worden opgemerkt dat wanneer het bedrag van BP groot is, het gemakkelijk is om te leiden tot de onderste laag van lichte afscherming.<\/p>\n

 <\/p>\n

BP heeft veel gesubstitueerde derivaten die effectieve fotoinitiatoren zijn, het belangrijkste derivaat is Michler's keton (MK), dat een 4,4-bis (dialkylamino) substituent is van BP, de algemene structuur wordt getoond in de linker figuur.<\/p>\n

Michler keton ten opzichte van BP, absorberen licht golflengte rood-verschoven tientallen nanometers, heeft een sterke absorptie van 365nm ultraviolet licht. Omdat het tertiaire amine structuur, dus michanone kan ook worden gebruikt als een fotoinitiator alleen, maar de effici\u00ebntie is niet volledig ontwikkeld. Zoals MK en BP gebruikt in combinatie met de fotopolymerisatie van acrylaten, bleek dat de initiatie activiteit veel hoger is dan MK \/ tertiaire amine systeem en BP \/ tertiaire amine systeem, de polymerisatiesnelheid is ongeveer 10 keer de laatste twee.<\/p>\n

Ten tweede, thioxanthrone + tertiair amine fotoinitiatiesysteem<\/p>\n

Thioxanthoon wordt ook gebruikt als waterstofgreep fotoinitiator, en de maximale absorptiegolflengte kan 380 ~ 420 nm bereiken, en de extinctieco\u00ebffici\u00ebnt is ook hoger, ongeveer 102 orden van grootte, die volledig gebruik kan maken van de lichtgolfenergie van 365 nm en 405 nm van de lichtbron, die veel effectiever is dan benzofenon fotoinitiator. In termen van initiatiemechanisme is het fotoinitiatorsysteem van thioxanthrone vergelijkbaar met het benzofenonsysteem. De structuurformules van thioxanthoon (TX) en zijn verschillende derivaten worden hieronder getoond.<\/p>\n

 <\/p>\n

Thioxanthon is een lichtgeel poeder met een zeer slechte oplosbaarheid in de meeste oplosmiddelen, waardoor het moeilijk te dispergeren is in harssystemen. De meeste hebben goede oplosbaarheids- en dispersie-eigenschappen en de absorptie en fotochemische activiteit kunnen worden verbeterd. De gebruikelijke gesubstitueerde TX zijn onder andere 2-chloorthianthrone (CTX), CPTX, isopropylthioanthrone (ITX) en 2,4-diethylthioanthrone (DETX). CTX is nog steeds niet goed oplosbaar en is geleidelijk vervangen door de laatste twee.<\/p>\n

De thianthrone substituenten moeten gekoppeld worden aan geschikte actieve amines om een effici\u00ebnte fotoinitierende activiteit te verkrijgen. Het bleek dat ethyl-4-dimethylaminobenzoaat (EDAB) de meest geschikte reactieve amineco-initiator is voor gebruik met thianthrone, dat niet alleen zeer actief is maar ook minder ernstige vergeling heeft. ITX is op grote schaal geaccepteerd door de markt vanwege de relatief goede kosten.<\/p>\n

 <\/p>\n

<\/h2>\n

Neem nu contact met ons op!<\/b><\/strong><\/h2>\n

Als je Price nodig hebt, vul dan je contactgegevens in op het formulier hieronder. We nemen dan meestal binnen 24 uur contact met je op. Je kunt me ook een e-mail sturen info@longchangchemical.com<\/a><\/span>\u00a0tijdens kantooruren (8:30 tot 18:00 UTC+8 ma. ~ za.) of gebruik de live chat op de website voor een snel antwoord.<\/b><\/strong><\/h4>\n

 <\/p>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
Fotoinitiator TPO<\/span><\/a><\/td>\nCAS 75980-60-8<\/td>\n<\/tr>\n
Fotoinitiator TMO<\/span><\/a><\/td>\nCAS 270586-78-2<\/td>\n<\/tr>\n
Fotoinitiator PD-01<\/span><\/a><\/td>\nCAS 579-07-7<\/td>\n<\/tr>\n
Fotoinitiator PBZ<\/span><\/a><\/td>\nCAS 2128-93-0<\/td>\n<\/tr>\n
Fotoinitiator OXE-02<\/span><\/a><\/td>\nCAS 478556-66-0<\/td>\n<\/tr>\n
Fotoinitiator OMBB<\/span><\/a><\/td>\nCAS 606-28-0<\/td>\n<\/tr>\n
Fotoinitiator MPBZ (6012)<\/span><\/a><\/td>\nCAS 86428-83-3<\/td>\n<\/tr>\n
Fotoinitiator MBP<\/span><\/a><\/td>\nCAS 134-84-9<\/td>\n<\/tr>\n
Fotoinitiator MBF<\/span><\/a><\/td>\nCAS 15206-55-0<\/td>\n<\/tr>\n
Fotoinitiator LAP<\/span><\/a><\/td>\nCAS 85073-19-4<\/td>\n<\/tr>\n
Fotoinitiator ITX<\/span><\/a><\/td>\nCAS 5495-84-1<\/td>\n<\/tr>\n
Fotoinitiator EMK<\/span><\/a><\/td>\nCAS 90-93-7<\/td>\n<\/tr>\n
Fotoinitiator EHA<\/span><\/a><\/td>\nCAS 21245-02-3<\/td>\n<\/tr>\n
Fotoinitiator EDB<\/span><\/a><\/td>\nCAS 10287-53-3<\/td>\n<\/tr>\n
Fotoinitiator DETX<\/span><\/a><\/td>\nCAS 82799-44-8<\/td>\n<\/tr>\n
Fotoinitiator CQ \/ Kamferchinon<\/span><\/a><\/td>\nCAS 10373-78-1<\/td>\n<\/tr>\n
Fotoinitiator CBP<\/span><\/a><\/td>\nCAS 134-85-0<\/td>\n<\/tr>\n
Fotoinitiator BP \/ Benzofenon<\/span><\/a><\/td>\nCAS 119-61-9<\/td>\n<\/tr>\n
Fotoinitiator BMS<\/span><\/a><\/td>\nCAS 83846-85-9<\/td>\n<\/tr>\n
Fotoinitiator 938<\/span><\/a><\/td>\nCAS 61358-25-6<\/td>\n<\/tr>\n
Fotoinitiator 937<\/span><\/a><\/td>\nCAS 71786-70-4<\/td>\n<\/tr>\n
Fotoinitiator 819 DW<\/span><\/a><\/td>\nCAS 162881-26-7<\/td>\n<\/tr>\n
Fotoinitiator 819<\/span><\/a><\/td>\nCAS 162881-26-7<\/td>\n<\/tr>\n
Fotoinitiator 784<\/span><\/a><\/td>\nCAS 125051-32-3<\/td>\n<\/tr>\n
Fotoinitiator 754<\/span><\/a><\/td>\nCAS 211510-16-6 442536-99-4<\/td>\n<\/tr>\n
Fotoinitiator 6993<\/span><\/a><\/td>\nCAS 71449-78-0<\/td>\n<\/tr>\n
Fotoinitiator 6976<\/span><\/a><\/td>\nCAS 71449-78-0 89452-37-9 108-32-7<\/td>\n<\/tr>\n
Fotoinitiator 379<\/span><\/a><\/td>\nCAS 119344-86-4<\/td>\n<\/tr>\n
Fotoinitiator 369<\/span><\/a><\/td>\nCAS 119313-12-1<\/td>\n<\/tr>\n
Fotoinitiator 160<\/a><\/span><\/td>\nCAS 71868-15-0<\/td>\n<\/tr>\n
Fotoinitiator 1206<\/span><\/a><\/td>\n<\/td>\n<\/tr>\n
Fotoinitiator 1173<\/span><\/a><\/td>\nCAS 7473-98-5<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n

 <\/p>","protected":false},"excerpt":{"rendered":"

Brief description of hydrogen-capturing photoinitiators and their two main categories Hydrogen-capturing photoinitiators, also known as type II photoinitiators, are generally dominated by aromatic ketone structures and also include certain thick-ringed aromatic hydrocarbons. They have certain light-absorbing properties, and the matching co-initiator, i.e. hydrogen donor, itself has no absorption in the long-wave UV range. 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