{"id":5398,"date":"2022-07-22T13:06:56","date_gmt":"2022-07-22T13:06:56","guid":{"rendered":"https:\/\/longchangchemical.com\/?p=5398"},"modified":"2024-12-11T15:40:41","modified_gmt":"2024-12-11T15:40:41","slug":"selection-of-photoinitiators-in-uv-coating-formulations","status":"publish","type":"post","link":"https:\/\/longchangchemical.com\/id\/selection-of-photoinitiators-in-uv-coating-formulations\/","title":{"rendered":"Pemilihan inisiator foto dalam formulasi pelapisan UV"},"content":{"rendered":"

Pemilihan inisiator foto dalam formulasi pelapisan UV<\/strong><\/h1>\n

Photoinisiator radikal bebas dibagi menjadi dua kategori utama menurut mekanisme kerja photoinisiator untuk menghasilkan radikal aktif, yaitu photoinisiator radikal bebas tipe pembelahan (juga dikenal sebagai photoinisiator tipe I), dan photoinisiator radikal bebas tipe penangkap hidrogen (juga dikenal sebagai photoinisiator tipe II). Fotoinisiator tipe pembelahan yang umum digunakan sebagian besar adalah aril alkil keton dari sudut pandang struktural, nilai yang umum adalah 184, 2959, 651, 907, 369, 1173, 819, TPO, MBF, 754, dll. Photoinisiator penangkap hidrogen yang umum digunakan sebagian besar adalah benzofenon atau keton aromatik heterosiklik dari sudut pandang struktural, dengan nilai umum seperti BP, ITX, dan 2-EA. Inisiator bersama yang umum adalah amina reaktif dan benzoat amina tersier. Artikel ini akan menggabungkan kinerja fotoinisiator dan kasus penggunaan untuk menjelaskan secara singkat pemilihan fotoinisiator dalam formulasi pelapis pengawet cahaya (UV).<\/p>\n

 <\/p>\n

Pertama<\/strong>spektrum serapan dari photoinisiator dan prinsip pencocokan spektrum emisi sumber cahaya.<\/p>\n

 <\/p>\n

Sumber cahaya yang tersedia secara komersial adalah lampu merkuri, lampu LED, lampu induksi dan lampu halida logam. Dalam pemilihan photoinisiator, menurut spektrum emisi sumber cahaya untuk memilih penyerapan spektrum inisiator yang lebih besar.<\/p>\n

<\/p>\n

 <\/p>\n

Contoh aplikasi. Dalam formulasi cat kuku, tabung lampu kuku yang umum digunakan adalah lampu neon dan lampu LED. Lampu neon memiliki spektrum emisi 370-420nm dan lampu LED memiliki spektrum emisi sekitar 365nm\/395nm. Kedua spektrum emisi lampu tersebut termasuk dalam wilayah panjang gelombang panjang dan memerlukan pemilihan inisiator yang menyerap cahaya pada panjang gelombang yang lebih panjang. Karena Tabel 1 menunjukkan puncak penyerapan berbagai photoinitiator yang umum, jika Anda ingin mencapai efek inisiasi yang diinginkan, Anda harus memilih photoinitiator dengan puncak penyerapan di atas 365nm, seperti TPO, 819, dll. Dalam pengujian aktual, semua efek pengawetan fotoinisiator TPO dan 819 bagus, dan efek yang diprediksi konsisten.<\/p>\n

 <\/p>\n

Kedua<\/strong>sistem berwarna, pemilihan photoinisiator pengawetan dalam sistem berwarna.<\/p>\n

 <\/p>\n

Pada sistem berwarna, terutama sistem gelap, pigmen itu sendiri akan menyerap sebagian energi UV, sehingga sinar UV tidak dapat menembus film cat, lapisan dalam photoinitiator tidak dapat menyerap energi yang cukup untuk memicu polimerisasi, dan pada akhirnya menyebabkan pengawetan yang buruk. Semakin ringan film, semakin rendah daya rekatnya, semakin serius kerutan pada permukaan, yang mempengaruhi sifat fisik dan kimiawi film cat. Dalam proses light curing, semakin panjang panjang gelombang sinar ultraviolet, semakin kuat penetrasinya dan semakin mudah mencapai lapisan film yang lebih dalam, sedangkan gelombang pendek tidak mudah mencapai lapisan film yang lebih dalam. Hal ini menyulitkan inisiasi polimerisasi atau pengawetan yang tidak sempurna pada lapisan yang lebih dalam dari film cat jika tidak ada inisiator foto gelombang panjang untuk menyerap energi dari gelombang panjang. Oleh karena itu, dalam sistem berwarna, pilihan fotoinisiator yang dalam sangat penting. Mengacu pada Tabel 1 di atas, photoinitiator gelombang panjang seperti TPO\/819\/651 dapat dipilih untuk bekerja lebih baik dengan photoinitiator gelombang pendek seperti 184\/1173.<\/p>\n

 <\/p>\n

Seperti pada cat warna satu lapis UV, sistem warna hitam rentan terhadap daya rekat yang buruk dan fenomena cat yang rontok dari kisi-kisi 100. Setelah menambahkan 1,5% 819 ke dalam formulasi, daya rekat lapisan cat meningkat secara signifikan, yang mengindikasikan bahwa 819 berperan sebagai fasilitator untuk pengawetan yang dalam. Selain itu, pada sistem hitam\/putih, senyawa 907\/ITX+184 dan senyawa 369\/ITX+184, efeknya luar biasa.<\/p>\n

 <\/p>\n

Ketiga<\/strong>ada persyaratan untuk pemilihan photoinisiator sistem pengawetan cahaya yang menguning.<\/p>\n

 <\/p>\n

Pada sistem pernis dan putih, ketahanan menguning merupakan indikator penting dari kinerja film cat, selain pemilihan ketahanan menguning yang baik dari resin, monomer, photoinisiator yang membawa masalah menguning juga perlu diperhatikan. Kehadiran substituen seperti itu dalam struktur konjugat fotoinisiator seperti N-dimetilamina akan menghasilkan kecenderungan yang lebih tinggi untuk menyinari menguning; demikian pula kehadiran substituen seperti itu dalam struktur amina aktif juga akan menyebabkan peningkatan penguningan.<\/p>\n

<\/p>\n

Tabel 2 di sebelah kiri menunjukkan perbandingan indeks penguningan berbagai formulasi photoinitiator setelah pemadatan dengan pentaeritritol triakrilat propoksida sebagai bahan utama dan tanpa photoinitiator sebagai referensi kosong. Seperti yang dapat dilihat dari tabel, 184, 1173, 754, MBF adalah photoinisiator yang tidak terlalu menguning, untuk pilihan utama pernis dan formulasi sistem putih.<\/p>\n

 <\/p>\n

Keempat<\/strong>kinerja kelarutan dalam pengencer dan oligomer aktif.<\/p>\n

<\/p>\n

Kelarutan yang baik merupakan prasyarat penting untuk pemilihan fotoinisiator dalam formulasi, semakin baik kompatibilitasnya, semakin stabil sistem formulasi. Seperti yang ditunjukkan pada gambar di sebelah kiri adalah kelarutan beberapa fotoinisiator dalam pelarut dan monomer yang umum.<\/p>\n

 <\/p>\n

Kelima<\/strong>pilihan inisiator foto UV-LED.<\/p>\n

Sumber cahaya UV-LED adalah peralatan curing yang berkembang pesat dalam beberapa tahun terakhir, karena hemat energi dan ramah lingkungan, tidak merusak substrat yang sangat populer, sehingga dalam curing UV-LED dalam pemilihan photoinisiator juga semakin diperhatikan penggunaannya. Formulasi curing UV-LED dalam pemilihan fotoinisiator juga harus dikombinasikan dengan prinsip-prinsip yang disebutkan di atas, pertama-tama, untuk memilih puncak penyerapan dan spektrum emisi sumber cahaya yang sesuai dengan fotoinisiator.<\/p>\n

Spektrum emisi sumber cahaya UV-LED antara 360-405nm, pada 365nm, 375nm, 385nm, 395nm, 405nm pada intensitas tertinggi, ini termasuk ke dalam wilayah gelombang panjang, sebaiknya memprioritaskan penggunaan photoinisiator gelombang panjang. Melalui pengujian lebih lanjut, beberapa photoinisiator dengan tingkat penyerapan tertinggi ditemukan masing-masing pada 365nm, 385nm dan 395nm. Dari segi efikasi, DETX dan EMK adalah photoinisiator yang sesuai untuk sumber cahaya UV-LED.<\/p>\n

<\/h4>\n

Inisiator Foto UV<\/span><\/a> Produk seri yang sama<\/strong><\/h2>\n

Hubungi Kami Sekarang!<\/b><\/strong><\/h2>\n

Jika Anda membutuhkan Harga, silakan isi informasi kontak Anda di formulir di bawah ini, kami biasanya akan menghubungi Anda dalam waktu 24 jam. Anda juga bisa mengirim email kepada saya info@longchangchemical.com<\/a><\/span>\u00a0selama jam kerja (8:30 pagi hingga 6:00 sore UTC+8 Senin-Sabtu) atau gunakan obrolan langsung situs web untuk mendapatkan balasan secepatnya.<\/b><\/strong><\/h4>\n

 <\/p>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
TPO pemrakarsa foto<\/span><\/a><\/td>\nCAS 75980-60-8<\/td>\n<\/tr>\n
Pemrakarsa foto TMO<\/span><\/a><\/td>\nCAS 270586-78-2<\/td>\n<\/tr>\n
Pemrakarsa foto PD-01<\/span><\/a><\/td>\nCAS 579-07-7<\/td>\n<\/tr>\n
Pemrakarsa foto PBZ<\/span><\/a><\/td>\nCAS 2128-93-0<\/td>\n<\/tr>\n
Pemrakarsa foto OXE-02<\/span><\/a><\/td>\nCAS 478556-66-0<\/td>\n<\/tr>\n
Pemrakarsa foto OMBB<\/span><\/a><\/td>\nCAS 606-28-0<\/td>\n<\/tr>\n
Pemrakarsa foto MPBZ (6012)<\/span><\/a><\/td>\nCAS 86428-83-3<\/td>\n<\/tr>\n
Pemrakarsa foto MBP<\/span><\/a><\/td>\nCAS 134-84-9<\/td>\n<\/tr>\n
Pemrakarsa foto MBF<\/span><\/a><\/td>\nCAS 15206-55-0<\/td>\n<\/tr>\n
PAPAN inisiator foto<\/span><\/a><\/td>\nCAS 85073-19-4<\/td>\n<\/tr>\n
Pemrakarsa foto ITX<\/span><\/a><\/td>\nCAS 5495-84-1<\/td>\n<\/tr>\n
Pemrakarsa foto EMK<\/span><\/a><\/td>\nCAS 90-93-7<\/td>\n<\/tr>\n
Pemrakarsa foto EHA<\/span><\/a><\/td>\nCAS 21245-02-3<\/td>\n<\/tr>\n
Pemrakarsa foto EDB<\/span><\/a><\/td>\nCAS 10287-53-3<\/td>\n<\/tr>\n
Pemrakarsa foto DETX<\/span><\/a><\/td>\nCAS 82799-44-8<\/td>\n<\/tr>\n
Pemrakarsa foto CQ \/ Kamperquinon<\/span><\/a><\/td>\nCAS 10373-78-1<\/td>\n<\/tr>\n
Pemrakarsa foto CBP<\/span><\/a><\/td>\nCAS 134-85-0<\/td>\n<\/tr>\n
Pemrakarsa foto BP \/ Benzofenon<\/span><\/a><\/td>\nCAS 119-61-9<\/td>\n<\/tr>\n
BMS inisiator foto<\/span><\/a><\/td>\nCAS 83846-85-9<\/td>\n<\/tr>\n
Pemrakarsa foto 938<\/span><\/a><\/td>\nCAS 61358-25-6<\/td>\n<\/tr>\n
Pemrakarsa foto 937<\/span><\/a><\/td>\nCAS 71786-70-4<\/td>\n<\/tr>\n
Pemrakarsa foto 819 DW<\/span><\/a><\/td>\nCAS 162881-26-7<\/td>\n<\/tr>\n
Pemrakarsa Foto 819<\/span><\/a><\/td>\nCAS 162881-26-7<\/td>\n<\/tr>\n
Pemrakarsa foto 784<\/span><\/a><\/td>\nCAS 125051-32-3<\/td>\n<\/tr>\n
Pemrakarsa foto 754<\/span><\/a><\/td>\nCAS 211510-16-6 442536-99-4<\/td>\n<\/tr>\n
Pemrakarsa foto 6993<\/span><\/a><\/td>\nCAS 71449-78-0<\/td>\n<\/tr>\n
Pemrakarsa foto 6976<\/span><\/a><\/td>\nCAS 71449-78-0 89452-37-9 108-32-7<\/td>\n<\/tr>\n
Pemrakarsa foto 379<\/span><\/a><\/td>\nCAS 119344-86-4<\/td>\n<\/tr>\n
Pemrakarsa foto 369<\/span><\/a><\/td>\nCAS 119313-12-1<\/td>\n<\/tr>\n
Pemrakarsa Foto 160<\/a><\/span><\/td>\nCAS 71868-15-0<\/td>\n<\/tr>\n
Pemrakarsa Foto 1206<\/span><\/a><\/td>\n<\/td>\n<\/tr>\n
Pemrakarsa foto 1173<\/span><\/a><\/td>\nCAS 7473-98-5<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n

 <\/p>","protected":false},"excerpt":{"rendered":"

Pemilihan fotoinisiator dalam formulasi pelapisan UV Fotoinisiator radikal bebas dibagi menjadi dua kategori utama sesuai dengan mekanisme kerja fotoinisiator untuk menghasilkan radikal aktif, yaitu fotoinisiator radikal bebas tipe pembelahan (juga dikenal sebagai fotoinisiator tipe I), dan fotoinisiator radikal bebas tipe penangkapan hidrogen (juga dikenal sebagai fotoinisiator tipe II). Umumnya [...]<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[114],"tags":[],"class_list":["post-5398","post","type-post","status-publish","format-standard","hentry","category-catalysts-chemical-auxiliary-agents"],"yoast_head":"\nSelection of photoinitiators in UV coating formulations - Longchang Chemical<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangchemical.com\/id\/selection-of-photoinitiators-in-uv-coating-formulations\/\" \/>\n<meta property=\"og:locale\" content=\"id_ID\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Selection of photoinitiators in UV coating formulations - Longchang Chemical\" \/>\n<meta property=\"og:description\" content=\"Selection of photoinitiators in UV coating formulations Free radical photoinitiators are divided into two main categories according to the mechanism of action of the photoinitiator to produce active radicals, namely cleavage type free radical photoinitiators (also known as type I photoinitiators), and hydrogen capture type free radical photoinitiators (also known as type II photoinitiators). 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